Food, feed and beverage · TD-NMR

Oil and moisture in seeds and nuts

Oilseeds, kernels and nuts can be measured for oil content and moisture whole, without grinding, drying or solvent, so the sample stays available for other uses.

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What it tells you

The value of a seed lot

The oil content of a seed lot decides what it is worth: what is paid to the grower, how much oil a crushing plant will recover, and how well a breeding line is performing. Moisture decides whether a lot can be stored safely and how much drying it needs.

Whole seeds in a tube are measured for oil content and moisture and stay intact afterwards
Whole seeds measured without being destroyed. Schematic illustration.
Typical samples

Where it is used

  • Rapeseed and canola, sunflower, soybean and flax
  • Cottonseed, castor and other oilseeds
  • Peanuts, almonds, hazelnuts and other nuts and kernels
  • Oilseed meal and press cake, including their residual oil

Typical tasks are paying for a delivery by quality, sorting lots when they arrive at a crushing plant, selecting breeding lines, and checking meal and cake.

Four steps from breeding to purchasing, plant intake and quality control, all using the same measurement
Where seed analysis is used along the chain. Schematic illustration.
How it works

Pour in, measure, read

The seeds are poured into a sample holder as they are. Oil and water give separate signals that fade at different speeds, so one measurement gives both results. A calibration for each crop turns the signals into percentages. Larger sample volumes are available for coarse materials such as nuts.

Methods and standards

Recognised reference methods

  • ISO 10565 for oilseeds and ISO 10632 for oilseed residues
  • AOCS Ak 4-95
  • Grain inspection procedures used in the United States

The reference extraction method for the oil content of oilseeds is ISO 659. It is the method against which the NMR calibration is made, and it is not an NMR method itself. Which of these documents applies depends on your market and your trade partners, and should be confirmed before a method is set up.

Why time-domain NMR

What it adds

  • No grinding, no drying oven and no solvent
  • The seeds are not destroyed, so the same sample can go on to other tests
  • Whole seeds of irregular shape can be measured as they are
  • A short measurement time suits intake and breeding work, where many samples arrive
  • Simple enough for routine staff to run
Good to know

Points that matter in practice

  • Make a calibration for each crop, and check whether varieties or growing regions need their own
  • Seed temperature and moisture affect the reading, so keep the conditions consistent
  • A result is only as good as the sample, so take representative samples from mixed lots
  • Very small samples, down to a few seeds, need a dedicated set-up and must be validated separately
  • Results should be compared with the reference extraction method as part of the calibration, and checked at regular intervals
How MSY Consulting helps

From your seeds to a routine method

Send or bring representative samples. MSY Consulting runs feasibility measurements, plans the calibration for your crops, compares the results with your reference method, and trains your team until the measurement is part of your routine.

Contact

Let's talk about your application

Send an email describing your instrument and your application, and you will get a reply.

contact@msyconsulting.eu

MSY CONSULTING SAS · Wissembourg, France · LinkedIn